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1coi

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(New page: 200px<br /><applet load="1coi" size="450" color="white" frame="true" align="right" spinBox="true" caption="1coi, resolution 2.1&Aring;" /> '''DESIGNED TRIMERIC COI...)
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[[Image:1coi.jpg|left|200px]]<br /><applet load="1coi" size="350" color="white" frame="true" align="right" spinBox="true"
caption="1coi, resolution 2.1&Aring;" />
caption="1coi, resolution 2.1&Aring;" />
'''DESIGNED TRIMERIC COILED COIL-VALD'''<br />
'''DESIGNED TRIMERIC COILED COIL-VALD'''<br />
==Overview==
==Overview==
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The three-dimensional structure of the 29-residue designed coiled coil, having the amino acid sequence acetyl-E VEALEKK VAALESK VQALEKK, VEALEHG-amide has been determined and refined to a crystallographic, R-factor of 21.4% for all data from 10-A to 2.1-A resolution. This, molecule is called coil-VaLd because it contains valine in the a heptad, positions and leucine in the d heptad positions. In the trigonal crystal, three molecules, related by a crystallographic threefold axis, form a, parallel three-helix bundle. The bundles are stacked head-to-tail to form, a continuous coiled coil along the c-direction of the crystal. The, contacts among the three helices within the coiled coil are mainly, hydrophobic: four layers of valine residues alternate with four layers of, leucine residues to form the core of the bundle. In contrast, mostly, hydrophilic contacts mediate the interaction between trimers: here a total, of two direct protein--protein hydrogen bonds are found. Based on the, structure, we propose a scheme for designing crystals of peptides, containing continuous two-, three-, and four-stranded coiled coils.
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The three-dimensional structure of the 29-residue designed coiled coil having the amino acid sequence acetyl-E VEALEKK VAALESK VQALEKK VEALEHG-amide has been determined and refined to a crystallographic R-factor of 21.4% for all data from 10-A to 2.1-A resolution. This molecule is called coil-VaLd because it contains valine in the a heptad positions and leucine in the d heptad positions. In the trigonal crystal, three molecules, related by a crystallographic threefold axis, form a parallel three-helix bundle. The bundles are stacked head-to-tail to form a continuous coiled coil along the c-direction of the crystal. The contacts among the three helices within the coiled coil are mainly hydrophobic: four layers of valine residues alternate with four layers of leucine residues to form the core of the bundle. In contrast, mostly hydrophilic contacts mediate the interaction between trimers: here a total of two direct protein--protein hydrogen bonds are found. Based on the structure, we propose a scheme for designing crystals of peptides containing continuous two-, three-, and four-stranded coiled coils.
==About this Structure==
==About this Structure==
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1COI is a [http://en.wikipedia.org/wiki/Protein_complex Protein complex] structure of sequences from [http://en.wikipedia.org/wiki/Synthetic_construct Synthetic construct] with SO4, ACE and NH2 as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://ispc.weizmann.ac.il/oca-bin/ocashort?id=1COI OCA].
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1COI is a [http://en.wikipedia.org/wiki/Protein_complex Protein complex] structure of sequences from [http://en.wikipedia.org/wiki/Synthetic_construct Synthetic construct] with <scene name='pdbligand=SO4:'>SO4</scene>, <scene name='pdbligand=ACE:'>ACE</scene> and <scene name='pdbligand=NH2:'>NH2</scene> as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1COI OCA].
==Reference==
==Reference==
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[[Category: Protein complex]]
[[Category: Protein complex]]
[[Category: Synthetic construct]]
[[Category: Synthetic construct]]
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[[Category: Degrado, W.F.]]
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[[Category: Degrado, W F.]]
[[Category: Eisenberg, D.]]
[[Category: Eisenberg, D.]]
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[[Category: Ogihara, N.L.]]
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[[Category: Ogihara, N L.]]
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[[Category: Weiss, M.S.]]
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[[Category: Weiss, M S.]]
[[Category: ACE]]
[[Category: ACE]]
[[Category: NH2]]
[[Category: NH2]]
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[[Category: protein design]]
[[Category: protein design]]
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''Page seeded by [http://ispc.weizmann.ac.il/oca OCA ] on Sun Nov 25 01:44:58 2007''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Feb 21 12:08:07 2008''

Revision as of 10:08, 21 February 2008


1coi, resolution 2.1Å

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DESIGNED TRIMERIC COILED COIL-VALD

Overview

The three-dimensional structure of the 29-residue designed coiled coil having the amino acid sequence acetyl-E VEALEKK VAALESK VQALEKK VEALEHG-amide has been determined and refined to a crystallographic R-factor of 21.4% for all data from 10-A to 2.1-A resolution. This molecule is called coil-VaLd because it contains valine in the a heptad positions and leucine in the d heptad positions. In the trigonal crystal, three molecules, related by a crystallographic threefold axis, form a parallel three-helix bundle. The bundles are stacked head-to-tail to form a continuous coiled coil along the c-direction of the crystal. The contacts among the three helices within the coiled coil are mainly hydrophobic: four layers of valine residues alternate with four layers of leucine residues to form the core of the bundle. In contrast, mostly hydrophilic contacts mediate the interaction between trimers: here a total of two direct protein--protein hydrogen bonds are found. Based on the structure, we propose a scheme for designing crystals of peptides containing continuous two-, three-, and four-stranded coiled coils.

About this Structure

1COI is a Protein complex structure of sequences from Synthetic construct with , and as ligands. Full crystallographic information is available from OCA.

Reference

The crystal structure of the designed trimeric coiled coil coil-VaLd: implications for engineering crystals and supramolecular assemblies., Ogihara NL, Weiss MS, Degrado WF, Eisenberg D, Protein Sci. 1997 Jan;6(1):80-8. PMID:9007979

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