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==Overview==
==Overview==
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The membrane protein squalene-hopene cyclase was cocrystallized with, 2-azasqualene and analyzed by X-ray diffraction to 2.13 A resolution. The, conformation of this close analog was clearly established, and it agreed, with the common textbook presentation. The bound squalene undergoes only, small conformational changes during the formation of rings A through D, thus requiring no intermediate. However, ring E formation is hindered by, an entropic barrier, which may explain its absence in the steroids. The, structure analysis revealed a mobile region between the active center, cavity and the membrane, which may melt, opening a passage for squalene, and hopene.
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The membrane protein squalene-hopene cyclase was cocrystallized with 2-azasqualene and analyzed by X-ray diffraction to 2.13 A resolution. The conformation of this close analog was clearly established, and it agreed with the common textbook presentation. The bound squalene undergoes only small conformational changes during the formation of rings A through D, thus requiring no intermediate. However, ring E formation is hindered by an entropic barrier, which may explain its absence in the steroids. The structure analysis revealed a mobile region between the active center cavity and the membrane, which may melt, opening a passage for squalene and hopene.
==About this Structure==
==About this Structure==
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[[Category: Squalene--hopene cyclase]]
[[Category: Squalene--hopene cyclase]]
[[Category: Balliano, G.]]
[[Category: Balliano, G.]]
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[[Category: Reinert, D.J.]]
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[[Category: Reinert, D J.]]
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[[Category: Schulz, G.E.]]
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[[Category: Schulz, G E.]]
[[Category: C8E]]
[[Category: C8E]]
[[Category: SQA]]
[[Category: SQA]]
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[[Category: triterpene cyclase]]
[[Category: triterpene cyclase]]
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Sun Feb 3 10:02:50 2008''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Feb 21 15:26:09 2008''

Revision as of 13:26, 21 February 2008


1ump, resolution 2.13Å

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GEOMETRY OF TRITERPENE CONVERSION TO PENTACARBOCYCLIC HOPENE

Overview

The membrane protein squalene-hopene cyclase was cocrystallized with 2-azasqualene and analyzed by X-ray diffraction to 2.13 A resolution. The conformation of this close analog was clearly established, and it agreed with the common textbook presentation. The bound squalene undergoes only small conformational changes during the formation of rings A through D, thus requiring no intermediate. However, ring E formation is hindered by an entropic barrier, which may explain its absence in the steroids. The structure analysis revealed a mobile region between the active center cavity and the membrane, which may melt, opening a passage for squalene and hopene.

About this Structure

1UMP is a Single protein structure of sequence from Alicyclobacillus acidocaldarius with and as ligands. Active as Squalene--hopene cyclase, with EC number 5.4.99.17 Known structural/functional Site: . Full crystallographic information is available from OCA.

Reference

Conversion of squalene to the pentacarbocyclic hopene., Reinert DJ, Balliano G, Schulz GE, Chem Biol. 2004 Jan;11(1):121-6. PMID:15113001

Page seeded by OCA on Thu Feb 21 15:26:09 2008

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