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5dva

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'''Unreleased structure'''
 
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The entry 5dva is ON HOLD until Paper Publication
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==Fragments bound to the OXA-48 beta-lactamase: Compound 1==
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<StructureSection load='5dva' size='340' side='right' caption='[[5dva]], [[Resolution|resolution]] 2.50&Aring;' scene=''>
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== Structural highlights ==
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<table><tr><td colspan='2'>[[5dva]] is a 4 chain structure. Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=5DVA OCA]. For a <b>guided tour on the structure components</b> use [http://oca.weizmann.ac.il/oca-docs/fgij/fg.htm?mol=5DVA FirstGlance]. <br>
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</td></tr><tr id='ligand'><td class="sblockLbl"><b>[[Ligand|Ligands:]]</b></td><td class="sblockDat"><scene name='pdbligand=5FL:3-(PYRIDIN-4-YL)BENZOIC+ACID'>5FL</scene>, <scene name='pdbligand=CL:CHLORIDE+ION'>CL</scene></td></tr>
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<tr id='NonStdRes'><td class="sblockLbl"><b>[[Non-Standard_Residue|NonStd Res:]]</b></td><td class="sblockDat"><scene name='pdbligand=KCX:LYSINE+NZ-CARBOXYLIC+ACID'>KCX</scene></td></tr>
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<tr id='related'><td class="sblockLbl"><b>[[Related_structure|Related:]]</b></td><td class="sblockDat">[[4s2p|4s2p]]</td></tr>
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<tr id='activity'><td class="sblockLbl"><b>Activity:</b></td><td class="sblockDat"><span class='plainlinks'>[http://en.wikipedia.org/wiki/Beta-lactamase Beta-lactamase], with EC number [http://www.brenda-enzymes.info/php/result_flat.php4?ecno=3.5.2.6 3.5.2.6] </span></td></tr>
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<tr id='resources'><td class="sblockLbl"><b>Resources:</b></td><td class="sblockDat"><span class='plainlinks'>[http://oca.weizmann.ac.il/oca-docs/fgij/fg.htm?mol=5dva FirstGlance], [http://oca.weizmann.ac.il/oca-bin/ocaids?id=5dva OCA], [http://pdbe.org/5dva PDBe], [http://www.rcsb.org/pdb/explore.do?structureId=5dva RCSB], [http://www.ebi.ac.uk/pdbsum/5dva PDBsum]</span></td></tr>
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</table>
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<div style="background-color:#fffaf0;">
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== Publication Abstract from PubMed ==
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The spread of antibiotic resistant bacteria is a global threat that shakes the foundations of modern healthcare. beta-Lactamases are enzymes that confer resistance to beta-lactam antibiotics in bacteria, and there is a critical need for new inhibitors of these enzymes for combination therapy together with an antibiotic. With this in mind, we have screened a library of 490 fragments to identify starting points for the development of new inhibitors of the class D beta-lactamase oxacillinase-48 (OXA-48) through surface plasmon resonance (SPR), dose-rate inhibition assays, and X-ray crystallography. Furthermore, we have uncovered structure-activity relationships and used alternate conformations from a crystallographic structure to grow a fragment into a more potent compound with a KD of 50 muM and an IC50 of 18 muM.
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Authors: Lund, B.A., Christopeit, T., Leiros, H.-K.S.
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Screening and Design of Inhibitor Scaffolds for the Antibiotic Resistance Oxacillinase-48 (OXA-48) through Surface Plasmon Resonance Screening.,Lund BA, Christopeit T, Guttormsen Y, Bayer A, Leiros HS J Med Chem. 2016 May 20. PMID:27165692<ref>PMID:27165692</ref>
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Description: Fragments bound to the OXA-48 beta-lactamase: Compound 1
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From MEDLINE&reg;/PubMed&reg;, a database of the U.S. National Library of Medicine.<br>
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[[Category: Unreleased Structures]]
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</div>
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[[Category: Leiros, H.-K.S]]
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<div class="pdbe-citations 5dva" style="background-color:#fffaf0;"></div>
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== References ==
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<references/>
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__TOC__
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</StructureSection>
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[[Category: Beta-lactamase]]
[[Category: Christopeit, T]]
[[Category: Christopeit, T]]
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[[Category: Lund, B.A]]
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[[Category: Leiros, H K.S]]
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[[Category: Lund, B A]]
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[[Category: Complex]]
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[[Category: Fragment]]
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[[Category: Hydrolase]]
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[[Category: Inhibitor]]
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[[Category: Lactamase]]

Revision as of 15:39, 1 June 2016

Fragments bound to the OXA-48 beta-lactamase: Compound 1

5dva, resolution 2.50Å

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