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===Structure===
===Structure===
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The class B GPCRs, including GCGR, are different from other GPCRs in several ways. The first is that class B GPCRs contain a protrusion known as a 'stalk,' a three α-helical turn elongation of the N-terminus that protrudes past the extracellular (EC) membrane. Structural integrity of this domain in GCGR is <scene name='72/721552/Ligand_binding_interactions/1'>essential to ligand binding affinity</scene> in that A135P mutations effect stalk stability through the removal of an important salt bridge between Glu133-Lys136.
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The class B GPCRs, including GCGR, are different from other GPCRs in several ways. The first is that class B GPCRs contain a protrusion known as a 'stalk,' a three α-helical turn elongation of the N-terminus that protrudes past the extracellular (EC) membrane. Structural integrity of this domain in GCGR is <scene name='72/721552/Ligand_binding_interactions/1'>essential to ligand binding affinity</scene>. A135P mutations impact stalk stability by removing an important salt bridge between Glu133 - Lys136. A second difference between class B and other GPCRs is that the extracellular loop 1 (ECL1) is 3-4 times longer than comparable loops in class A GPCRs, and also affects ligand binding affinity.<ref name= "Siu 2013"/> Most notably, class B GPCRs contain a <scene name='72/727091/Corticotropin_glucagon_aligned/1'>prominent central splay</scene> which is solvent filled and accessible from the extracellular side. This central splay is notably absent <scene name='72/727091/B2-adrenergic_glucagon_aligned/9'>from other GPCRs</scene>, and represents a tantalizing target for agonists/antagonists.<ref name= "Hollenstein 2014"/>
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A second difference between class B and other GPCRs is that the extracellular loop 1 (ECL1) is 3-4 times longer than comparable loops in class A GPCRs, and also affects ligand binding affinity.<ref name= "Siu 2013"/>
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Most notably, class B GPCRs contain a <scene name='72/727091/Corticotropin_glucagon_aligned/1'>prominent central splay</scene> which is solvent filled and accessible from the extracellular side. This central splay is notably absent <scene name='72/727091/B2-adrenergic_glucagon_aligned/9'>from other GPCRs</scene>, and represents a tantalizing target for agonists/antagonists.<ref name= "Hollenstein 2014"/>
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Because of the difficulty in stabilizing and crystallizing Class B TMDs, very little is known about the conformational changes that transduce cell signals endogenously. GCGR is known to regulate additional signal pathways through the adoption of differing receptor conformations and to interact with receptor activity-modifying proteins (RAMPs) altering the signaling bias of the receptor.<ref name= "Xu 2009"/>
Because of the difficulty in stabilizing and crystallizing Class B TMDs, very little is known about the conformational changes that transduce cell signals endogenously. GCGR is known to regulate additional signal pathways through the adoption of differing receptor conformations and to interact with receptor activity-modifying proteins (RAMPs) altering the signaling bias of the receptor.<ref name= "Xu 2009"/>
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[[Image:Protter GLR HUMAN.png |400 px|left|thumb|Fig. 1: Snake Plot of GCGR TMD. Residues of particular importance in glucagon binding affinity are found in green, yellow, and black. Residues in red are the location of critical disulfide bonds, while blue residues were found to be highly conserved across all class B GPCRs.<ref name= "Siu 2013"/>]]
[[Image:Protter GLR HUMAN.png |400 px|left|thumb|Fig. 1: Snake Plot of GCGR TMD. Residues of particular importance in glucagon binding affinity are found in green, yellow, and black. Residues in red are the location of critical disulfide bonds, while blue residues were found to be highly conserved across all class B GPCRs.<ref name= "Siu 2013"/>]]
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In a comprehensive mutagenesis and glucagon-binding study, a total of 129 mutations were tested. 41 of these covering 28 different locations in the GCGR were found to have at least a fourfold decrease in glucagon binding affinity<ref name= "Siu 2013"/>. (see Fig. 1) It is the face of the central cavity that harbors the majority of the residues which play an important role in glucagon binding.<ref name= "Siu 2013"/> The binding site was shown to be a dynamic area traveling from the middle of the stalk region to deep within the 7TM core. (See Fig. 2) [[Image:Movie Frame 8.png |275 px|right|thumb|Fig. 2: Relationship between Tyr138 and Glu362 - residues spanning the height of the glucagon binding pocket in GCGR.]] The binding site encompasses positions along ECL1, ECL2 and ECL3 and helices I, II, III, V, VI and VII, while extending deep in the 7TM cavity.
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In a comprehensive mutagenesis and glucagon-binding study, a total of 129 mutations of GCGR were tested. 41 of these covering 28 different locations in the GCGR TMD were found to have at least a fourfold decrease in glucagon binding affinity<ref name= "Siu 2013"/>. (see Fig. 1) It is the face of the central cavity that harbors the majority of the residues which play an important role in glucagon binding.<ref name= "Siu 2013"/> The binding site was shown to be a dynamic area traveling from the middle of the stalk region (Tyr 138) to deep within the 7TM core (Glu 362), encompassing positions along ECL1, ECL2 and ECL3 and helices I, II, III, V, VI and VII.
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Mutagenesis and photo cross-linking studies determined essential, conserved residues in glucagon and have been <scene name='72/727091/Glucagon_important_residues/2'>labeled and colored</scene> in red.<ref name= "Siu 2013"/> Glucagon residues His 1, Gln 3, Phe 6, and Tyr 10 are critical to successful binding interaction with the GCGR while others are important for structural rigidity. The n-terminal random coil of glucagon (Fig. 2) leads to a protuberance that fits into the deep, interior cavity of the GCGR 7TM (Fig. 3). There is a <scene name='72/721552/Glucagon_binding_zoomed_in/1'>narrow neck</scene> to the entrance of the cavity, providing a firm anchor during peptide docking.
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[[Image:Glucagon with Q3 and N-terminus.png |200 px|right|thumb|Fig. 2: Surface visualization of glucagon visualizing the three dimensional shape of the N-terminal tail that interacts with the binding site of GCGR central cavity.]]
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[[Image:Movie Frame 6.png |200 px|right|thumb|Fig. 3: Ballooned pocket functioning as anchoring site for <scene name='72/721552/Glucagon_binding/3'>glucagon's n-terminal residues</scene>.]]
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Glucagon itself carries <scene name='72/727091/Glucagon_important_residues/2'>several residues</scene> essential to the proper binding of glucagon to the GCGR. Residues His 1, Gln 3, Phe 6, and Tyr 10 are critical to successful ligand
 
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Essential, conserved residues of glucagon, as discovered through mutagenesis and photo cross-linking studies have been labeled and colored in red. <ref name= "Siu 2013"/>
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Through mutagenesis and photo-crosslinking studies, several residues deep within the central cavity of the GCGR 7TMD were discovered neighboring Glu362, which is approximately 19 angstroms from the base of the EC stalk and the location of Tyr138. (Fig. 8)
Through mutagenesis and photo-crosslinking studies, several residues deep within the central cavity of the GCGR 7TMD were discovered neighboring Glu362, which is approximately 19 angstroms from the base of the EC stalk and the location of Tyr138. (Fig. 8)
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<scene name='72/721552/Glucagon_binding/3'>Glucagon Binding Full Rendering</scene>
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Four essential residues exist deep within the central cavity which all play strong roles in ligand binding affinity. (Fig. 9)
Four essential residues exist deep within the central cavity which all play strong roles in ligand binding affinity. (Fig. 9)
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<scene name='72/721552/Glucagon_binding_zoomed_in/1'>Glucagon Binding Zoomed in</scene>
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A narrow entry gives way to a large, anchoring site for residues 1-4 of glucagon. (Fig. 10)
A narrow entry gives way to a large, anchoring site for residues 1-4 of glucagon. (Fig. 10)
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[[Image:Movie Frame 6.png |100 px|left|thumb|Fig. 10: Ballooned pocket functioning as anchoring site for glucagon residues 1-4.]]
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[[Image:Glucagon with Q3 and N-terminus.png |275 px|right|thumb|Fig. 11: Surface visualization of glucagon demonstrating three dimensional fit of N-terminal tail into binding site of GCGR central cavity active site]]
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==Clinical relevance==
==Clinical relevance==

Revision as of 22:36, 21 April 2016

Glucagon G protein-coupled receptor

PDB ID 4L6R

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