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1fzd

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(New page: 200px<br /> <applet load="1fzd" size="450" color="white" frame="true" align="right" spinBox="true" caption="1fzd, resolution 2.1&Aring;" /> '''STRUCTURE OF RECOMBI...)
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<applet load="1fzd" size="450" color="white" frame="true" align="right" spinBox="true"
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caption="1fzd, resolution 2.1&Aring;" />
'''STRUCTURE OF RECOMBINANT ALPHAEC DOMAIN FROM HUMAN FIBRINOGEN-420'''<br />
'''STRUCTURE OF RECOMBINANT ALPHAEC DOMAIN FROM HUMAN FIBRINOGEN-420'''<br />
==Overview==
==Overview==
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The crystal structure of a recombinant alphaEC domain from human, fibrinogen-420 has been determined at a resolution of 2.1 A. The protein, which corresponds to the carboxyl domain of the alphaE chain, was, expressed in and purified from Pichia pastoris cells. Felicitously, during, crystallization an amino-terminal segment was removed, apparently by a, contaminating protease, allowing the 201-residue remaining parent body to, crystallize. An x-ray structure was determined by molecular replacement., The electron density was clearly defined, partly as a result of averaging, made possible by there being eight molecules in the asymmetric unit, related by noncrystallographic symmetry (P1 space group). Virtually all of, an asparagine-linked sugar cluster is present. Comparison with structures, of the beta- and gamma-chain carboxyl domains of human fibrinogen revealed, that the binding cleft is essentially neutral and should not bind, Gly-Pro-Arg or Gly-His-Arg peptides of the sort bound by those other, domains. Nonetheless, the cleft is clearly evident, and the possibility of, binding a carbohydrate ligand like sialic acid has been considered.
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The crystal structure of a recombinant alphaEC domain from human fibrinogen-420 has been determined at a resolution of 2.1 A. The protein, which corresponds to the carboxyl domain of the alphaE chain, was expressed in and purified from Pichia pastoris cells. Felicitously, during crystallization an amino-terminal segment was removed, apparently by a contaminating protease, allowing the 201-residue remaining parent body to crystallize. An x-ray structure was determined by molecular replacement. The electron density was clearly defined, partly as a result of averaging made possible by there being eight molecules in the asymmetric unit related by noncrystallographic symmetry (P1 space group). Virtually all of an asparagine-linked sugar cluster is present. Comparison with structures of the beta- and gamma-chain carboxyl domains of human fibrinogen revealed that the binding cleft is essentially neutral and should not bind Gly-Pro-Arg or Gly-His-Arg peptides of the sort bound by those other domains. Nonetheless, the cleft is clearly evident, and the possibility of binding a carbohydrate ligand like sialic acid has been considered.
==Disease==
==Disease==
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==About this Structure==
==About this Structure==
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1FZD is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Homo_sapiens Homo sapiens] with NAG and CA as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://ispc.weizmann.ac.il/oca-bin/ocashort?id=1FZD OCA].
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1FZD is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Homo_sapiens Homo sapiens] with <scene name='pdbligand=NAG:'>NAG</scene> and <scene name='pdbligand=CA:'>CA</scene> as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1FZD OCA].
==Reference==
==Reference==
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[[Category: Single protein]]
[[Category: Single protein]]
[[Category: Applegate, D.]]
[[Category: Applegate, D.]]
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[[Category: Doolittle, R.F.]]
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[[Category: Doolittle, R F.]]
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[[Category: Everse, S.J.]]
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[[Category: Everse, S J.]]
[[Category: Grieninger, G.]]
[[Category: Grieninger, G.]]
[[Category: Redman, C.]]
[[Category: Redman, C.]]
[[Category: Spraggon, G.]]
[[Category: Spraggon, G.]]
[[Category: Veerapandian, L.]]
[[Category: Veerapandian, L.]]
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[[Category: Zhang, J.Z.]]
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[[Category: Zhang, J Z.]]
[[Category: CA]]
[[Category: CA]]
[[Category: NAG]]
[[Category: NAG]]
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[[Category: glycosylated protein]]
[[Category: glycosylated protein]]
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''Page seeded by [http://ispc.weizmann.ac.il/oca OCA ] on Mon Nov 12 16:58:45 2007''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Feb 21 12:44:19 2008''

Revision as of 10:44, 21 February 2008


1fzd, resolution 2.1Å

Drag the structure with the mouse to rotate

STRUCTURE OF RECOMBINANT ALPHAEC DOMAIN FROM HUMAN FIBRINOGEN-420

Contents

Overview

The crystal structure of a recombinant alphaEC domain from human fibrinogen-420 has been determined at a resolution of 2.1 A. The protein, which corresponds to the carboxyl domain of the alphaE chain, was expressed in and purified from Pichia pastoris cells. Felicitously, during crystallization an amino-terminal segment was removed, apparently by a contaminating protease, allowing the 201-residue remaining parent body to crystallize. An x-ray structure was determined by molecular replacement. The electron density was clearly defined, partly as a result of averaging made possible by there being eight molecules in the asymmetric unit related by noncrystallographic symmetry (P1 space group). Virtually all of an asparagine-linked sugar cluster is present. Comparison with structures of the beta- and gamma-chain carboxyl domains of human fibrinogen revealed that the binding cleft is essentially neutral and should not bind Gly-Pro-Arg or Gly-His-Arg peptides of the sort bound by those other domains. Nonetheless, the cleft is clearly evident, and the possibility of binding a carbohydrate ligand like sialic acid has been considered.

Disease

Known diseases associated with this structure: Afibrinogenemia, congenital OMIM:[134820], Amyloidosis, hereditary renal OMIM:[134820], Dysfibrinogenemia, alpha type, causing bleeding diathesis OMIM:[134820], Dysfibrinogenemia, alpha type, causing recurrent thrombosis OMIM:[134820]

About this Structure

1FZD is a Single protein structure of sequence from Homo sapiens with and as ligands. Full crystallographic information is available from OCA.

Reference

Crystal structure of a recombinant alphaEC domain from human fibrinogen-420., Spraggon G, Applegate D, Everse SJ, Zhang JZ, Veerapandian L, Redman C, Doolittle RF, Grieninger G, Proc Natl Acad Sci U S A. 1998 Aug 4;95(16):9099-104. PMID:9689040

Page seeded by OCA on Thu Feb 21 12:44:19 2008

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