1hne

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'''STRUCTURE OF HUMAN NEUTROPHIL ELASTASE IN COMPLEX WITH A PEPTIDE CHLOROMETHYL KETONE INHIBITOR AT 1.84-ANGSTROMS RESOLUTION'''<br />
'''STRUCTURE OF HUMAN NEUTROPHIL ELASTASE IN COMPLEX WITH A PEPTIDE CHLOROMETHYL KETONE INHIBITOR AT 1.84-ANGSTROMS RESOLUTION'''<br />
==Overview==
==Overview==
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Human neutrophil elastase (HNE) has been implicated as a major contributor, to tissue destruction in various disease states, including emphysema. The, structure of HNE, at neutral pH, in complex with, methoxysuccinyl-Ala-Ala-Pro-Ala chloromethyl ketone (MSACK), has been, solved and refined to an R factor of 16.4% at 1.84-A resolution. Results, are consistent with the currently accepted mechanism of peptide, chloromethyl ketone inhibition of serine proteases, in that MSACK, cross-links the catalytic residues His-57 and Ser-195. The structure of, the HNE-MSACK complex is compared with that of porcine pancreatic elastase, in complex with L-647,957, a beta-lactam inhibitor of both elastases. The, distribution of positively charged residues on HNE is highly asymmetric, and may play a role in its specific association with the underlying, negatively charged proteoglycan matrix of the neutrophil granules in which, the enzyme is stored.
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Human neutrophil elastase (HNE) has been implicated as a major contributor to tissue destruction in various disease states, including emphysema. The structure of HNE, at neutral pH, in complex with methoxysuccinyl-Ala-Ala-Pro-Ala chloromethyl ketone (MSACK), has been solved and refined to an R factor of 16.4% at 1.84-A resolution. Results are consistent with the currently accepted mechanism of peptide chloromethyl ketone inhibition of serine proteases, in that MSACK cross-links the catalytic residues His-57 and Ser-195. The structure of the HNE-MSACK complex is compared with that of porcine pancreatic elastase in complex with L-647,957, a beta-lactam inhibitor of both elastases. The distribution of positively charged residues on HNE is highly asymmetric and may play a role in its specific association with the underlying negatively charged proteoglycan matrix of the neutrophil granules in which the enzyme is stored.
==Disease==
==Disease==
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==About this Structure==
==About this Structure==
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1HNE is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/ ]. Active as [http://en.wikipedia.org/wiki/Leukocyte_elastase Leukocyte elastase], with EC number [http://www.brenda-enzymes.info/php/result_flat.php4?ecno=3.4.21.37 3.4.21.37] Full crystallographic information is available from [http://ispc.weizmann.ac.il/oca-bin/ocashort?id=1HNE OCA].
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1HNE is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/ ]. Active as [http://en.wikipedia.org/wiki/Leukocyte_elastase Leukocyte elastase], with EC number [http://www.brenda-enzymes.info/php/result_flat.php4?ecno=3.4.21.37 3.4.21.37] Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1HNE OCA].
==Reference==
==Reference==
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[[Category: Leukocyte elastase]]
[[Category: Leukocyte elastase]]
[[Category: Single protein]]
[[Category: Single protein]]
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[[Category: Dorn, C.P.]]
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[[Category: Dorn, C P.]]
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[[Category: Fluder, E.M.]]
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[[Category: Fluder, E M.]]
[[Category: Hoogsteen, K.]]
[[Category: Hoogsteen, K.]]
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[[Category: Lin, T.Y.]]
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[[Category: Lin, T Y.]]
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[[Category: Mckeever, B.M.]]
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[[Category: Mckeever, B M.]]
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[[Category: Navia, M.A.]]
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[[Category: Navia, M A.]]
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[[Category: Springer, J.P.]]
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[[Category: Springer, J P.]]
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[[Category: Williams, H.R.]]
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[[Category: Williams, H R.]]
[[Category: hydrolase(serine proteinase)]]
[[Category: hydrolase(serine proteinase)]]
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Feb 21 13:02:58 2008''

Revision as of 11:02, 21 February 2008


1hne, resolution 1.84Å

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STRUCTURE OF HUMAN NEUTROPHIL ELASTASE IN COMPLEX WITH A PEPTIDE CHLOROMETHYL KETONE INHIBITOR AT 1.84-ANGSTROMS RESOLUTION

Contents

Overview

Human neutrophil elastase (HNE) has been implicated as a major contributor to tissue destruction in various disease states, including emphysema. The structure of HNE, at neutral pH, in complex with methoxysuccinyl-Ala-Ala-Pro-Ala chloromethyl ketone (MSACK), has been solved and refined to an R factor of 16.4% at 1.84-A resolution. Results are consistent with the currently accepted mechanism of peptide chloromethyl ketone inhibition of serine proteases, in that MSACK cross-links the catalytic residues His-57 and Ser-195. The structure of the HNE-MSACK complex is compared with that of porcine pancreatic elastase in complex with L-647,957, a beta-lactam inhibitor of both elastases. The distribution of positively charged residues on HNE is highly asymmetric and may play a role in its specific association with the underlying negatively charged proteoglycan matrix of the neutrophil granules in which the enzyme is stored.

Disease

Known diseases associated with this structure: Hematopoiesis, cyclic OMIM:[130130], Neutropenia, congenital OMIM:[130130]

About this Structure

1HNE is a Single protein structure of sequence from [1]. Active as Leukocyte elastase, with EC number 3.4.21.37 Full crystallographic information is available from OCA.

Reference

Structure of human neutrophil elastase in complex with a peptide chloromethyl ketone inhibitor at 1.84-A resolution., Navia MA, McKeever BM, Springer JP, Lin TY, Williams HR, Fluder EM, Dorn CP, Hoogsteen K, Proc Natl Acad Sci U S A. 1989 Jan;86(1):7-11. PMID:2911584

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