1q7o

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[[Image:1q7o.jpg|left|200px]]
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{{Seed}}
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{{STRUCTURE_1q7o| PDB=1q7o | SCENE= }}
{{STRUCTURE_1q7o| PDB=1q7o | SCENE= }}
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'''Determination of f-MLF-OH Peptide Structure with solid-state magic-angle spinning NMR Spectroscopy'''
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===Determination of f-MLF-OH Peptide Structure with solid-state magic-angle spinning NMR Spectroscopy===
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==Overview==
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The three-dimensional structure of the chemotactic peptide N-formyl-l-Met-l-Leu-l-Phe-OH was determined by using solid-state NMR (SSNMR). The set of SSNMR data consisted of 16 (13)C-(15)N distances and 18 torsion angle constraints (on 10 angles), recorded from uniformly (13)C,(15)N- and (15)N-labeled samples. The peptide's structure was calculated by means of simulated annealing and a newly developed protocol that ensures that all of conformational space, consistent with the structural constraints, is searched completely. The result is a high-quality structure of a molecule that has thus far not been amenable to single-crystal diffraction studies. The extensions of the SSNMR techniques and computational methods to larger systems appear promising.
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The line below this paragraph, {{ABSTRACT_PUBMED_12149447}}, adds the Publication Abstract to the page
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(as it appears on PubMed at http://www.pubmed.gov), where 12149447 is the PubMed ID number.
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{{ABSTRACT_PUBMED_12149447}}
==About this Structure==
==About this Structure==
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Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1Q7O OCA].
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Full experimental information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1Q7O OCA].
==Reference==
==Reference==
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[[Category: Chemotactic peptide]]
[[Category: Chemotactic peptide]]
[[Category: Mlf]]
[[Category: Mlf]]
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Sat May 3 05:58:13 2008''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Mon Jul 28 09:24:28 2008''

Revision as of 06:24, 28 July 2008

Image:1q7o.png

Template:STRUCTURE 1q7o

Determination of f-MLF-OH Peptide Structure with solid-state magic-angle spinning NMR Spectroscopy

Template:ABSTRACT PUBMED 12149447

About this Structure

Full experimental information is available from OCA.

Reference

De novo determination of peptide structure with solid-state magic-angle spinning NMR spectroscopy., Rienstra CM, Tucker-Kellogg L, Jaroniec CP, Hohwy M, Reif B, McMahon MT, Tidor B, Lozano-Perez T, Griffin RG, Proc Natl Acad Sci U S A. 2002 Aug 6;99(16):10260-5. Epub 2002 Jul 29. PMID:12149447

Page seeded by OCA on Mon Jul 28 09:24:28 2008

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