1pu7

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(New page: 200px<br /><applet load="1pu7" size="450" color="white" frame="true" align="right" spinBox="true" caption="1pu7, resolution 1.93&Aring;" /> '''Crystal structure of...)
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caption="1pu7, resolution 1.93&Aring;" />
'''Crystal structure of H.pylori 3-methyladenine DNA glycosylase (MagIII) bound to 3,9-dimethyladenine'''<br />
'''Crystal structure of H.pylori 3-methyladenine DNA glycosylase (MagIII) bound to 3,9-dimethyladenine'''<br />
==Overview==
==Overview==
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DNA glycosylases catalyze the excision of chemically modified bases from, DNA. Although most glycosylases are specific to a particular base, the, 3-methyladenine (m3A) DNA glycosylases include both highly specific, enzymes acting on a single modified base, and enzymes with broader, specificity for alkylation-damaged DNA. Our structural understanding of, these different enzymatic specificities is currently limited to crystal, and NMR structures of the unliganded enzymes and complexes with abasic DNA, inhibitors. Presented here are high-resolution crystal structures of the, m3A DNA glycosylase from Helicobacter pylori (MagIII) in the unliganded, form and bound to alkylated bases 3,9-dimethyladenine and, 1,N6-ethenoadenine. These are the first structures of a nucleobase bound, in the active site of a m3A glycosylase belonging to the, helix-hairpin-helix superfamily. MagIII achieves its specificity for, positively-charged m3A not by direct interactions with purine or methyl, substituent atoms, but rather by stacking the base between two aromatic, side chains in a pocket that excludes 7-methylguanine. We report base, excision and DNA binding activities of MagIII active site mutants, together with a structural comparison of the HhH glycosylases.
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DNA glycosylases catalyze the excision of chemically modified bases from DNA. Although most glycosylases are specific to a particular base, the 3-methyladenine (m3A) DNA glycosylases include both highly specific enzymes acting on a single modified base, and enzymes with broader specificity for alkylation-damaged DNA. Our structural understanding of these different enzymatic specificities is currently limited to crystal and NMR structures of the unliganded enzymes and complexes with abasic DNA inhibitors. Presented here are high-resolution crystal structures of the m3A DNA glycosylase from Helicobacter pylori (MagIII) in the unliganded form and bound to alkylated bases 3,9-dimethyladenine and 1,N6-ethenoadenine. These are the first structures of a nucleobase bound in the active site of a m3A glycosylase belonging to the helix-hairpin-helix superfamily. MagIII achieves its specificity for positively-charged m3A not by direct interactions with purine or methyl substituent atoms, but rather by stacking the base between two aromatic side chains in a pocket that excludes 7-methylguanine. We report base excision and DNA binding activities of MagIII active site mutants, together with a structural comparison of the HhH glycosylases.
==About this Structure==
==About this Structure==
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1PU7 is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Helicobacter_pylori Helicobacter pylori] with 39A and BME as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://ispc.weizmann.ac.il/oca-bin/ocashort?id=1PU7 OCA].
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1PU7 is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Helicobacter_pylori Helicobacter pylori] with <scene name='pdbligand=39A:'>39A</scene> and <scene name='pdbligand=BME:'>BME</scene> as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1PU7 OCA].
==Reference==
==Reference==
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[[Category: Helicobacter pylori]]
[[Category: Helicobacter pylori]]
[[Category: Single protein]]
[[Category: Single protein]]
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[[Category: Eichman, B.F.]]
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[[Category: Eichman, B F.]]
[[Category: Ellenberger, T.]]
[[Category: Ellenberger, T.]]
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[[Category: Radicella, J.P.]]
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[[Category: Radicella, J P.]]
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[[Category: Rourke, E.J.O.]]
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[[Category: Rourke, E J.O.]]
[[Category: 39A]]
[[Category: 39A]]
[[Category: BME]]
[[Category: BME]]
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[[Category: helix-hairpin-helix]]
[[Category: helix-hairpin-helix]]
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''Page seeded by [http://ispc.weizmann.ac.il/oca OCA ] on Sun Nov 25 03:00:15 2007''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Feb 21 14:32:37 2008''

Revision as of 12:32, 21 February 2008


1pu7, resolution 1.93Å

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Crystal structure of H.pylori 3-methyladenine DNA glycosylase (MagIII) bound to 3,9-dimethyladenine

Overview

DNA glycosylases catalyze the excision of chemically modified bases from DNA. Although most glycosylases are specific to a particular base, the 3-methyladenine (m3A) DNA glycosylases include both highly specific enzymes acting on a single modified base, and enzymes with broader specificity for alkylation-damaged DNA. Our structural understanding of these different enzymatic specificities is currently limited to crystal and NMR structures of the unliganded enzymes and complexes with abasic DNA inhibitors. Presented here are high-resolution crystal structures of the m3A DNA glycosylase from Helicobacter pylori (MagIII) in the unliganded form and bound to alkylated bases 3,9-dimethyladenine and 1,N6-ethenoadenine. These are the first structures of a nucleobase bound in the active site of a m3A glycosylase belonging to the helix-hairpin-helix superfamily. MagIII achieves its specificity for positively-charged m3A not by direct interactions with purine or methyl substituent atoms, but rather by stacking the base between two aromatic side chains in a pocket that excludes 7-methylguanine. We report base excision and DNA binding activities of MagIII active site mutants, together with a structural comparison of the HhH glycosylases.

About this Structure

1PU7 is a Single protein structure of sequence from Helicobacter pylori with and as ligands. Full crystallographic information is available from OCA.

Reference

Crystal structures of 3-methyladenine DNA glycosylase MagIII and the recognition of alkylated bases., Eichman BF, O'Rourke EJ, Radicella JP, Ellenberger T, EMBO J. 2003 Oct 1;22(19):4898-909. PMID:14517230

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