1u8v

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(New page: 200px<br /><applet load="1u8v" size="450" color="white" frame="true" align="right" spinBox="true" caption="1u8v, resolution 1.6&Aring;" /> '''Crystal Structure of ...)
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[[Image:1u8v.jpg|left|200px]]<br /><applet load="1u8v" size="350" color="white" frame="true" align="right" spinBox="true"
caption="1u8v, resolution 1.6&Aring;" />
caption="1u8v, resolution 1.6&Aring;" />
'''Crystal Structure of 4-Hydroxybutyryl-CoA Dehydratase from Clostridium aminobutyricum: Radical catalysis involving a [4Fe-4S] cluster and flavin'''<br />
'''Crystal Structure of 4-Hydroxybutyryl-CoA Dehydratase from Clostridium aminobutyricum: Radical catalysis involving a [4Fe-4S] cluster and flavin'''<br />
==Overview==
==Overview==
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Dehydratases catalyze the breakage of a carbon-oxygen bond leading to, unsaturated products via the elimination of water. The 1.6-A resolution, crystal structure of 4-hydroxybutyryl-CoA dehydratase from the, gamma-aminobutyrate-fermenting Clostridium aminobutyricum represents a new, class of dehydratases with an unprecedented active site architecture. A, [4Fe-4S](2+) cluster, coordinated by three cysteine and one histidine, residues, is located 7 A from the Re-side of a flavin adenine dinucleotide, (FAD) moiety. The structure provides insight into the function of these, ubiquitous prosthetic groups in the chemically nonfacile, radical-mediated, dehydration of 4-hydroxybutyryl-CoA. The substrate can be bound between, the [4Fe-4S](2+) cluster and the FAD with both cofactors contributing to, its radical activation and catalytic conversion. Our results raise, interesting questions regarding the mechanism of acyl-CoA dehydrogenases, which are involved in fatty acid oxidation, and address the divergent, evolution of the ancestral common gene.
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Dehydratases catalyze the breakage of a carbon-oxygen bond leading to unsaturated products via the elimination of water. The 1.6-A resolution crystal structure of 4-hydroxybutyryl-CoA dehydratase from the gamma-aminobutyrate-fermenting Clostridium aminobutyricum represents a new class of dehydratases with an unprecedented active site architecture. A [4Fe-4S](2+) cluster, coordinated by three cysteine and one histidine residues, is located 7 A from the Re-side of a flavin adenine dinucleotide (FAD) moiety. The structure provides insight into the function of these ubiquitous prosthetic groups in the chemically nonfacile, radical-mediated dehydration of 4-hydroxybutyryl-CoA. The substrate can be bound between the [4Fe-4S](2+) cluster and the FAD with both cofactors contributing to its radical activation and catalytic conversion. Our results raise interesting questions regarding the mechanism of acyl-CoA dehydrogenases, which are involved in fatty acid oxidation, and address the divergent evolution of the ancestral common gene.
==About this Structure==
==About this Structure==
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1U8V is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Clostridium_aminobutyricum Clostridium aminobutyricum] with SF4 and FAD as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://ispc.weizmann.ac.il/oca-bin/ocashort?id=1U8V OCA].
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1U8V is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Clostridium_aminobutyricum Clostridium aminobutyricum] with <scene name='pdbligand=SF4:'>SF4</scene> and <scene name='pdbligand=FAD:'>FAD</scene> as [http://en.wikipedia.org/wiki/ligands ligands]. Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1U8V OCA].
==Reference==
==Reference==
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[[Category: Cinkaya, I.]]
[[Category: Cinkaya, I.]]
[[Category: Dobbek, H.]]
[[Category: Dobbek, H.]]
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[[Category: Martins, B.M.]]
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[[Category: Martins, B M.]]
[[Category: Messerschmidt, A.]]
[[Category: Messerschmidt, A.]]
[[Category: FAD]]
[[Category: FAD]]
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[[Category: beta-strands]]
[[Category: beta-strands]]
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''Page seeded by [http://ispc.weizmann.ac.il/oca OCA ] on Wed Nov 21 03:55:39 2007''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Feb 21 15:21:52 2008''

Revision as of 13:21, 21 February 2008


1u8v, resolution 1.6Å

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Crystal Structure of 4-Hydroxybutyryl-CoA Dehydratase from Clostridium aminobutyricum: Radical catalysis involving a [4Fe-4S] cluster and flavin

Overview

Dehydratases catalyze the breakage of a carbon-oxygen bond leading to unsaturated products via the elimination of water. The 1.6-A resolution crystal structure of 4-hydroxybutyryl-CoA dehydratase from the gamma-aminobutyrate-fermenting Clostridium aminobutyricum represents a new class of dehydratases with an unprecedented active site architecture. A [4Fe-4S](2+) cluster, coordinated by three cysteine and one histidine residues, is located 7 A from the Re-side of a flavin adenine dinucleotide (FAD) moiety. The structure provides insight into the function of these ubiquitous prosthetic groups in the chemically nonfacile, radical-mediated dehydration of 4-hydroxybutyryl-CoA. The substrate can be bound between the [4Fe-4S](2+) cluster and the FAD with both cofactors contributing to its radical activation and catalytic conversion. Our results raise interesting questions regarding the mechanism of acyl-CoA dehydrogenases, which are involved in fatty acid oxidation, and address the divergent evolution of the ancestral common gene.

About this Structure

1U8V is a Single protein structure of sequence from Clostridium aminobutyricum with and as ligands. Full crystallographic information is available from OCA.

Reference

Crystal structure of 4-hydroxybutyryl-CoA dehydratase: radical catalysis involving a [4Fe-4S] cluster and flavin., Martins BM, Dobbek H, Cinkaya I, Buckel W, Messerschmidt A, Proc Natl Acad Sci U S A. 2004 Nov 2;101(44):15645-9. Epub 2004 Oct 20. PMID:15496473

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