1zjk

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(New page: 200px<br /> <applet load="1zjk" size="450" color="white" frame="true" align="right" spinBox="true" caption="1zjk, resolution 2.18&Aring;" /> '''Crystal structure o...)
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<applet load="1zjk" size="450" color="white" frame="true" align="right" spinBox="true"
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caption="1zjk, resolution 2.18&Aring;" />
caption="1zjk, resolution 2.18&Aring;" />
'''Crystal structure of the zymogen catalytic region of human MASP-2'''<br />
'''Crystal structure of the zymogen catalytic region of human MASP-2'''<br />
==Overview==
==Overview==
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Few reports have described in detail a true autoactivation process, where, no extrinsic cleavage factors are required to initiate the autoactivation, of a zymogen. Herein, we provide structural and mechanistic insight into, the autoactivation of a multidomain serine protease: mannose-binding, lectin-associated serine protease-2 (MASP-2), the first enzymatic, component in the lectin pathway of complement activation. We characterized, the proenzyme form of a MASP-2 catalytic fragment encompassing its, C-terminal three domains and solved its crystal structure at 2.4 A, resolution. Surprisingly, zymogen MASP-2 is capable of cleaving its, natural substrate C4, with an efficiency about 10% that of active MASP-2., Comparison of the zymogen and active structures of MASP-2 reveals that, in, addition to the activation domain, other loops of the serine protease, domain undergo significant conformational changes. This additional, flexibility could play a key role in the transition of zymogen MASP-2 into, a proteolytically active form. Based on the three-dimensional structures, of proenzyme and active MASP-2 catalytic fragments, we present model for, the active zymogen MASP-2 complex and propose a mechanism for the, autoactivation process.
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Few reports have described in detail a true autoactivation process, where no extrinsic cleavage factors are required to initiate the autoactivation of a zymogen. Herein, we provide structural and mechanistic insight into the autoactivation of a multidomain serine protease: mannose-binding lectin-associated serine protease-2 (MASP-2), the first enzymatic component in the lectin pathway of complement activation. We characterized the proenzyme form of a MASP-2 catalytic fragment encompassing its C-terminal three domains and solved its crystal structure at 2.4 A resolution. Surprisingly, zymogen MASP-2 is capable of cleaving its natural substrate C4, with an efficiency about 10% that of active MASP-2. Comparison of the zymogen and active structures of MASP-2 reveals that, in addition to the activation domain, other loops of the serine protease domain undergo significant conformational changes. This additional flexibility could play a key role in the transition of zymogen MASP-2 into a proteolytically active form. Based on the three-dimensional structures of proenzyme and active MASP-2 catalytic fragments, we present model for the active zymogen MASP-2 complex and propose a mechanism for the autoactivation process.
==Disease==
==Disease==
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==About this Structure==
==About this Structure==
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1ZJK is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Homo_sapiens Homo sapiens]. Full crystallographic information is available from [http://ispc.weizmann.ac.il/oca-bin/ocashort?id=1ZJK OCA].
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1ZJK is a [http://en.wikipedia.org/wiki/Single_protein Single protein] structure of sequence from [http://en.wikipedia.org/wiki/Homo_sapiens Homo sapiens]. Full crystallographic information is available from [http://oca.weizmann.ac.il/oca-bin/ocashort?id=1ZJK OCA].
==Reference==
==Reference==
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[[Category: Kocsis, A.]]
[[Category: Kocsis, A.]]
[[Category: Naray-Szabo, G.]]
[[Category: Naray-Szabo, G.]]
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[[Category: Sim, R.B.]]
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[[Category: Sim, R B.]]
[[Category: Vegh, B.]]
[[Category: Vegh, B.]]
[[Category: Zavodszky, P.]]
[[Category: Zavodszky, P.]]
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[[Category: modular protein]]
[[Category: modular protein]]
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''Page seeded by [http://ispc.weizmann.ac.il/oca OCA ] on Mon Nov 12 20:35:28 2007''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Feb 21 16:16:17 2008''

Revision as of 14:16, 21 February 2008


1zjk, resolution 2.18Å

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Crystal structure of the zymogen catalytic region of human MASP-2

Contents

Overview

Few reports have described in detail a true autoactivation process, where no extrinsic cleavage factors are required to initiate the autoactivation of a zymogen. Herein, we provide structural and mechanistic insight into the autoactivation of a multidomain serine protease: mannose-binding lectin-associated serine protease-2 (MASP-2), the first enzymatic component in the lectin pathway of complement activation. We characterized the proenzyme form of a MASP-2 catalytic fragment encompassing its C-terminal three domains and solved its crystal structure at 2.4 A resolution. Surprisingly, zymogen MASP-2 is capable of cleaving its natural substrate C4, with an efficiency about 10% that of active MASP-2. Comparison of the zymogen and active structures of MASP-2 reveals that, in addition to the activation domain, other loops of the serine protease domain undergo significant conformational changes. This additional flexibility could play a key role in the transition of zymogen MASP-2 into a proteolytically active form. Based on the three-dimensional structures of proenzyme and active MASP-2 catalytic fragments, we present model for the active zymogen MASP-2 complex and propose a mechanism for the autoactivation process.

Disease

Known disease associated with this structure: MASP2 deficiency OMIM:[605102]

About this Structure

1ZJK is a Single protein structure of sequence from Homo sapiens. Full crystallographic information is available from OCA.

Reference

A true autoactivating enzyme. Structural insight into mannose-binding lectin-associated serine protease-2 activations., Gal P, Harmat V, Kocsis A, Bian T, Barna L, Ambrus G, Vegh B, Balczer J, Sim RB, Naray-Szabo G, Zavodszky P, J Biol Chem. 2005 Sep 30;280(39):33435-44. Epub 2005 Jul 21. PMID:16040602

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