1izc

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|PDB= 1izc |SIZE=350|CAPTION= <scene name='initialview01'>1izc</scene>, resolution 1.7&Aring;
|PDB= 1izc |SIZE=350|CAPTION= <scene name='initialview01'>1izc</scene>, resolution 1.7&Aring;
|SITE=
|SITE=
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|LIGAND= <scene name='pdbligand=MG:MAGNESIUM+ION'>MG</scene> and <scene name='pdbligand=PYR:PYRUVIC ACID'>PYR</scene>
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|LIGAND= <scene name='pdbligand=MG:MAGNESIUM+ION'>MG</scene>, <scene name='pdbligand=PYR:PYRUVIC+ACID'>PYR</scene>
|ACTIVITY=
|ACTIVITY=
|GENE=
|GENE=
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|DOMAIN=
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|RELATEDENTRY=
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|RESOURCES=<span class='plainlinks'>[http://oca.weizmann.ac.il/oca-docs/fgij/fg.htm?mol=1izc FirstGlance], [http://oca.weizmann.ac.il/oca-bin/ocaids?id=1izc OCA], [http://www.ebi.ac.uk/pdbsum/1izc PDBsum], [http://www.rcsb.org/pdb/explore.do?structureId=1izc RCSB]</span>
}}
}}
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[[Category: Watanabe, K.]]
[[Category: Watanabe, K.]]
[[Category: Yao, M.]]
[[Category: Yao, M.]]
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[[Category: MG]]
 
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[[Category: PYR]]
 
[[Category: pyruvate mg(ii) complex]]
[[Category: pyruvate mg(ii) complex]]
[[Category: tim-barrel]]
[[Category: tim-barrel]]
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Mar 20 11:57:00 2008''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Sun Mar 30 21:26:48 2008''

Revision as of 18:26, 30 March 2008


PDB ID 1izc

Drag the structure with the mouse to rotate
, resolution 1.7Å
Ligands: ,
Resources: FirstGlance, OCA, PDBsum, RCSB
Coordinates: save as pdb, mmCIF, xml



Crystal Structure Analysis of Macrophomate synthase


Overview

The Diels-Alder reaction, which forms a six-membered ring from an alkene (dienophile) and a 1,3-diene, is synthetically very useful for construction of cyclic products with high regio- and stereoselectivity under mild conditions. It has been applied to the synthesis of complex pharmaceutical and biologically active compounds. Although evidence on natural Diels-Alderases has been accumulated in the biosynthesis of secondary metabolites, there has been no report on the structural details of the natural Diels-Alderases. The function and catalytic mechanism of the natural Diels-Alderase are of great interest owing to the diversity of molecular skeletons in natural Diels-Alder adducts. Here we present the 1.70 A resolution crystal structure of the natural Diels-Alderase, fungal macrophomate synthase (MPS), in complex with pyruvate. The active site of the enzyme is large and hydrophobic, contributing amino acid residues that can hydrogen-bond to the substrate 2-pyrone. These data provide information on the catalytic mechanism of MPS, and suggest that the reaction proceeds via a large-scale structural reorganization of the product.

About this Structure

1IZC is a Single protein structure of sequence from Macrophoma commelinae. Full crystallographic information is available from OCA.

Reference

Insight into a natural Diels-Alder reaction from the structure of macrophomate synthase., Ose T, Watanabe K, Mie T, Honma M, Watanabe H, Yao M, Oikawa H, Tanaka I, Nature. 2003 Mar 13;422(6928):185-9. PMID:12634789

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