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2oqn

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|PDB= 2oqn |SIZE=350|CAPTION= <scene name='initialview01'>2oqn</scene>, resolution 1.90&Aring;
|PDB= 2oqn |SIZE=350|CAPTION= <scene name='initialview01'>2oqn</scene>, resolution 1.90&Aring;
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|LIGAND= <scene name='pdbligand=TAR:D(-)-TARTARIC ACID'>TAR</scene>
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|LIGAND= <scene name='pdbligand=TAR:D(-)-TARTARIC+ACID'>TAR</scene>
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|ACTIVITY=
|GENE=
|GENE=
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|RELATEDENTRY=
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|RESOURCES=<span class='plainlinks'>[http://oca.weizmann.ac.il/oca-docs/fgij/fg.htm?mol=2oqn FirstGlance], [http://oca.weizmann.ac.il/oca-bin/ocaids?id=2oqn OCA], [http://www.ebi.ac.uk/pdbsum/2oqn PDBsum], [http://www.rcsb.org/pdb/explore.do?structureId=2oqn RCSB]</span>
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[[Category: Hao, Q.]]
[[Category: Hao, Q.]]
[[Category: Kim, C U.]]
[[Category: Kim, C U.]]
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[[Category: TAR]]
 
[[Category: capillary cryoprotection]]
[[Category: capillary cryoprotection]]
[[Category: high pressure cryocooling]]
[[Category: high pressure cryocooling]]
[[Category: sulfur sad phasing]]
[[Category: sulfur sad phasing]]
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Thu Mar 20 18:03:17 2008''
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''Page seeded by [http://oca.weizmann.ac.il/oca OCA ] on Mon Mar 31 04:21:43 2008''

Revision as of 01:21, 31 March 2008


PDB ID 2oqn

Drag the structure with the mouse to rotate
, resolution 1.90Å
Ligands:
Resources: FirstGlance, OCA, PDBsum, RCSB
Coordinates: save as pdb, mmCIF, xml



High Pressure Cryocooling of Capillary Sample Cryoprotection and Diffraction Phasing at Long Wavelengths


Overview

Crystal cryocooling is usually employed to reduce radiation damage during X-ray crystallography. Recently, a high-pressure cryocooling method has been developed which results in excellent diffraction-quality crystals without the use of penetrative cryoprotectants. Three new developments of the method are presented here: (i) Xe-He high-pressure cryocooling for Xe SAD phasing, (ii) native sulfur SAD phasing and (iii) successful cryopreservation of crystals in thick-walled capillaries without additional cryoprotectants other than the native mother liquor. These developments may be useful for structural solution of proteins without the need for selenomethionine incorporation and for high-throughput protein crystallography.

About this Structure

2OQN is a Single protein structure of sequence from Thaumatococcus daniellii. Full crystallographic information is available from OCA.

Reference

High-pressure cryocooling for capillary sample cryoprotection and diffraction phasing at long wavelengths., Kim CU, Hao Q, Gruner SM, Acta Crystallogr D Biol Crystallogr. 2007 May;63(Pt 5):653-9. Epub 2007, Apr 21. PMID:17452791

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