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1hjg

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Revision as of 10:30, 30 October 2007 by OCA (Talk | contribs)
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1hjg, resolution 1.5Å

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ALTERATION OF THE CO-SUBSTRATE SELECTIVITY OF DEACETOXYCEPHALOSPORIN C SYNTHASE: THE ROLE OF ARGININE-258

Overview

Deacetoxycephalosporin C synthase is an iron(II) 2-oxoglutaratedependent, oxygenase that catalyzes the oxidative ring-expansion of penicillin N to, deacetoxycephalosporin C. The wild-type enzyme is only able to efficiently, utilize 2-oxoglutarate and 2-oxoadipate as a 2-oxoacid co-substrate., Mutation of arginine 258, the side chain of which forms an electrostatic, interaction with the 5-carboxylate of the 2-oxoglutarate co-substrate, to, a glutamine residue reduced activity to about 5% of the wild-type enzyme, with 2-oxoglutarate. However, other aliphatic 2-oxoacids, which were not, co-substrates for the wild-type enzyme, were utilized by the R258Q mutant., These 2-oxoacids "rescued" catalytic activity to the level observed for, the wild-type enzyme as judged by penicillin N and G ... [(full description)]

About this Structure

1HJG is a [Single protein] structure of sequence from [Streptomyces clavuligerus] with FE2 and KIV as [ligands]. Structure known Active Sites: FE and KIV. Full crystallographic information is available from [OCA].

Reference

Alteration of the co-substrate selectivity of deacetoxycephalosporin C synthase. The role of arginine 258., Lee HJ, Lloyd MD, Clifton IJ, Harlos K, Dubus A, Baldwin JE, Frere JM, Schofield CJ, J Biol Chem. 2001 May 25;276(21):18290-5. Epub 2001 Feb 21. PMID:11279000

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